Ke5frf, I understand what you are proposing, but it's a Rube Goldberg approach to the solution, when a simple current source will do the same thing with more precision and hands-off operation.
If it were my problem, I would continue trying a current source, and beat my head against the wall until it worked, because I know it should.
I totally agree that it is a clap-trap way of doing it, this is so at least with the modified suggestion I made with two timers and two potentiometers. The first suggestion, with one timer paralleled with the potentiometer, not so much...and I think it would work just as well. Only drawback is that when the timer circuit opens, the single potentiometer will have to be adjusted in such way to bring the current down significantly, and it will take just that much longer to get it to his target range.
But all of this got me to thinking, why isn't his CLD working? It should, if everything is set up right, and if I understand it correctly.
But then, I thought about the first stage of the process, when the distilled water is practically infinite in resistance. How different is the distilled water solution from any other insulator at this point? Is the resistance enough to keep any kind of current path from forming? Will the diode permit ANY current to flow without even the slightest path to ground? Perhaps its is like an AC motor that has to have a run capacitor to establish the momentum to make it run. I have a pretty good knowledge base, but I can't answer that question.
If I were there, I would set up the diode like it is supposed to be, and then read my voltage at the electrodes. If the diode is conducting at all, it should read 35 volts. If not, Perhaps his voltage is stopping at the anode? And because of this, the electrolysis process won't even kick start. But then, I considered the impedance of a voltmeter. Would it fool me if I read the voltage at the electrodes?...because even though the meter is high impedance, it may be low enough impedance to establish a path to ground and forward bias the diode.
So, between this thought experiment and the timer idea, I came up with an experiment I believe he should try.
He should set up his diode, ammeter, power supply, and electrodes in the series configuration as it should be, with fresh distilled water. But to start, he should use an alligator jumper to bypass the diode. The electrolysis should immediately begin. After the time he expects the current to reach 1 mA, he should disconnect his alligator jumper. At this stage the electrolyte solution should have a resistivity of 24kOhms on its own accord. If the diode works as I understand it, it should now be forward biased and conducting. it will see the "load resistance" of the electrolyte and adjust itself to begin limiting the current. As the process continues and the electrolyte becomes more conductive, the CLD SHOULD increase its resistance to make up the difference. In other words, if we help it get there in the first place, the diode should do its job.
If the experiment goes as I suggest it will, then it will be a simple matter of wiring up the diode in parallel with a timer switch, and setting the timer for the next test for the duration we experienced when the current reached 1 mA.
As I suggested before, all things being equal and assuming the purity of the distilled water is the same each time, the electrolysis process should have predictable time constraints, so a timer would be an effective way to kick start the procedure until the resistivity of the electrolyte is sufficient for the CLD to do its thing. He may even find the timer doesn't have to be set for long at all, as the conductivity of the electrolyte might be sufficient within an hour or less.
So, to sum it up, perhaps my original idea was Rube Goldbergish, but hopefully we can bear fruit with a simple modification to blend both methods together.